20-56 ASPECTE MORFOLOGICE ŞI STRUCTURALE ALE AMESTECULUI PULVERULENT Fe50Ni50 SUPUS ALIERII MECANICE


MORPHOLOGICAL AND STRUCTURAL ASPECTS
OF Fe50Ni50 POWDER MIXTURE SUBJECTED TO
MECHANICAL ALLOYING
The mechanical alloying experiment was performed inti a planetary
ball mill using elemental Fe and Ni powders mixed together at 50 wt. % ratio.
Powder samples were taken out after 1, 2, 4, 8, 16, 32, 48, and 64 hours of
milling. These samples were subjected to X-ray diffraction, sieving analysis,
and optical microscopy inspection. The results allow us to conclude that Ni
presents a ductile behaviour meanwhile Fe acts as a brittle component which
conducts to the forming of mixed particles of Ni embedding smaller Fe one. The
particle structure is more refined progressive with the milling time. Finally, the
solid solution of Fe in Ni FCC is completely formed at 64 hours of milling.
Keywords: Fe-Ni, alloy mechanical, planetary mill
Cuvinte cheie: Fe-Ni, aliere mecanică, moară planetară

56 ASPECTE MORFOLOGICE ŞI STRUCTURALE